Lamotte SMART3 Colorimeter User Manual Page 211
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- Table of contents
- TROUBLESHOOTING
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NICKEL
DIMETHYLGLYOXIME METHOD • CODE 3663-SC
QUANTITY CONTENTS CODE
60 mL *Hydrochloric Acid, 2.5N *6251PS-H
30 g *Ammonium Persulfate Reagent *6566-G
30 mL *Silver Nitrate Solution, 0.0141N *6346WT-G
250 mL Sodium Citrate, 10% 6253-K
60 mL *Dimethylglyoxime, 1% *6254-H
60 mL *Ammonium Hydroxide, Conc. *6537-H
3 Pipets, 1.0 mL, plastic 0354
1 Spoon, 0.1 g, plastic 0699
1 Test tube, 5-10-12.9-15-20-25, glass, w/cap 0608
1 Graduated Cylinder, 10 mL, glass 0416
*WARNING: Reagents marked with an * are considered to be potential health
hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents
go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail,
phone or fax.
Nickel is not usually found in natural waters except as a result of contamination
from industrial wastewaters as a corrosion product of stainless steel and nickel
alloys. Nickel may also enter surface waters from plating bath process water.
APPLICATION: Drinking and surface waters; domestic and industrial
wastewater.
RANGE: 0.00–8.00 ppm Nickel
MDL: 0.15 ppm
METHOD: Nickel under basic conditions forms a colored complex
with dimethylglyoxime in proportion to the concentration
of nickel.
SAMPLE HANDLING
& PRESERVATION:
Samples may be collected in either plastic or
glass containers and preserved by adding 5 mL of
concentrated nitric acid per liter.
INTERFERENCES: Organic matter interferes. Cobalt, iron, copper,
manganese and chromium do not interfere if each of the
concentrations is below 15 ppm.
SMART3 Test Procedures 11.10 NICKEL
Test Procedures
- CONTENTS 3
- GENERAL INFORMATION 5
- LIMITS OF LIABILITY 6
- WARRANTY 6
- REGISTER YOUR METER 6
- SPECIFICATIONS 7
- 6 SMART3 Colorimeter 11.10 8
- CONTENTS AND ACCESSORIES 9
- ACCESSORIES 9
- EPA COMPLIANCE 10
- CE COMPLIANCE 10
- IP67 CERTIFICATION 10
- CHEMICAL TESTING 11
- Sampling of Closed System 12
- FILTRATION 12
- SMART3 Colorimeter 11.10 11 13
- REAGENT BLANK 14
- METER CARE 14
- CALIBRATION 15
- CALIBRATION CURVES 15
- 14 SMART3 Colorimeter 11.10 16
- SMART3 Colorimeter 11.10 15 17
- STANDARD ADDITIONS 18
- MEASUREMENTS 19
- INTERFERENCES 20
- STRAY LIGHT INTERFERENCE 20
- OPERATION OF THE 21
- SMART3 COLORIMETER 21
- COMPONENTS 22
- GENERAL OPERATING PROCEDURES 23
- 22 SMART3 Colorimeter 11.10 24
- Result or 25
- LOOPING MENUS 26
- TESTING MENU 27
- TEST SEQUENCES 28
- GENERAL TESTING PROCEDURES 28
- 1.00 ppm 30
- SMART3 Colorimeter 11.10 29 31
- 0.28 ppm 32
- 0.30 ppm 33
- 32 SMART3 Colorimeter 11.10 34
- SMART3 Colorimeter 11.10 35 37
- EDITING MENU 38
- SMART3 Colorimeter 11.10 37 39
- Editing/Set Up 39
- ADDING OR DELETING A TEST 40
- ADDING A TEST 40
- DELETING A TEST 42
- SMART3 Colorimeter 11.10 41 43
- EDIT USER TESTS 44
- U V W X 46
- H I J K 46
- S T U V 47
- 2 3 4 5 47
- E P Q R 47
- O P Q R 47
- 46 SMART3 Colorimeter 11.10 48
- 0 1 2 3 50
- 1 1 2 3 50
- . – 0 1 51
- SMART3 Colorimeter 11.10 51 53
- 52 SMART3 Colorimeter 11.10 54
- – 1 2 3 55
- O 1 2 3 55
- . – 0 1 55
- SETTING THE CLOCK 59
- LOGGING DATA 60
- FACTORY SETUP 61
- SETTING POWER SAVE 61
- 60 SMART3 Colorimeter 11.10 62
- SETTING THE BACKLIGHT TIME 63
- SELECTING A LANGUAGE 64
- SMART3 Colorimeter 11.10 63 65
- COMPUTER CONNECTION 66
- BATTERY/AC OPERATION 67
- MAINTENANCE 68
- TROUBLESHOOTING 69
- TROUBLESHOOTING GUIDE 70
- 1910-TEST 71
- 02.13.12 71
- REAGENT SYSTEMS 73
- ALKALINITY–UDV 77
- ALUMINUM 79
- AMMONIA NITROGEN - LOW RANGE 81
- PROCEDURE - FRESH WATER 82
- PROCEDURE - SALT WATER 82
- AMMONIA NITROGEN - HIGH RANGE 84
- BENZOTRIAZOLE/TOLYLTRIAZOLE 89
- BENZOTRIAZOLE PROCEDURE 91
- TOLYLTRIAZOLE PROCEDURE 92
- BIGUANIDE 93
- BORATE - UDV 95
- PROCEDURE 100
- Test Procedures 101
- PROCEDURE A: 102
- BROMINE (NO CHLORINE) 102
- PROCEDURE B: 102
- PROCEDURE C: 103
- BROMINE - UDV 105
- PAN METHOD • CODE 4017-01 109
- CHLORIDE 111
- CHLORINE 113
- PROCEDURE–FREE CHLORINE 115
- PROCEDURE–TOTAL CHLORINE 115
- PROCEDURE–COMBINED CHLORINE 119
- CHLORINE, FREE - UDV 121
- CHLORINE, TOTAL - UDV 125
- CHLORINE DIOXIDE 129
- CHROMIUM, HEXAVALENT 131
- CHROMIUM - HEXAVALENT 133
- TRIVALENT & TOTAL 133
- HEXAVALENT CHROMIUM PROCEDURE 135
- TRIVALENT CHROMIUM PROCEDURE 136
- PAN METHOD · CODE 4851 137
- COD – LOW RANGE 139
- COD – STANDARD RANGE 143
- COD – HIGH RANGE 147
- PLATINUM COBALT METHOD 151
- NO REAGENTS REQUIRED 151
- COPPER – LOW RANGE 153
- CUPRIZONE METHOD • CODE 4023 155
- COPPER – UDV 159
- CODE 3660-01-SC 163
- CYANURIC ACID 167
- CYANURIC ACID – UDV 169
- DISSOLVED OXYGEN 173
- FLUORIDE 177
- HARDNESS, TOTAL – UDV 181
- HYDRAZINE 183
- HYDROGEN PEROXIDE – LOW RANGE 185
- DPD METHOD • CODE 4045-01 187
- HYDROGEN PEROXIDE – SHOCK 189
- IRON – UDV 195
- PAR METHOD · CODE 4031 201
- MANGANESE – LOW RANGE 203
- MANGANESE – HIGH RANGE 205
- TMK METHOD · CODE 4861 207
- PREPARATION OF *TMK INDICATOR 208
- MOLYBDENUM – HIGH RANGE 209
- NITRATE - UDV 215
- NITRATE-NITROGEN – LOW RANGE 219
- NITRITE-NITROGEN – LOW RANGE 223
- NITROGEN, TOTAL 225
- OXYGEN SCAVENGERS 229
- DEHA PROCEDURE 231
- CARBOHYDRAZIDE PROCEDURE 232
- ERYTHORBIC ACID PROCEDURE 233
- HYDROQUINONE PROCEDURE 234
- METHYLETHYLKETOXIME PROCEDURE 235
- DPD METHOD • CODE 4881 237
- PROCEDURE - OZONE ONLY 238
- INDIGO METHOD • CODE 3651-SC 241
- PROCEDURE–LOW RANGE 242
- PROCEDURE–HIGH RANGE 243
- PHOSPHATE – LOW RANGE 251
- PHOSPHATE – HIGH RANGE 255
- PHOSPHATE ppb 257
- PHOSPHORUS, TOTAL - LOW RANGE 261
- DIGESTION • CODE 4025-01 265
- POTASSIUM 269
- SILICA – LOW RANGE 271
- SILICA – HIGH RANGE 275
- SULFATE – HIGH RANGE 277
- SULFIDE – LOW RANGE 279
- SURFACTANTS 283
- CODE 3666-01-SC 285
- TURBIDITY 287
- ZINC – LOW RANGE 289
- APPENDIX 292
- Appendix 293
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